3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

Base Information

Chemical Name:3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline
CAS No.:1128112-41-3
Molecular Formula:C₂₈H₄₁NO₅Si
Molecular Weight:499.723
Hs Code.:

Synonyms:3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

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Chemical Property of 3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

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Technology Process of 3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

There total 1 articles about 3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1128112-89-9
N-{(1E)-[2-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]methylene}-3,4-dimethoxy-7-methylbicyclo[4.2.0]octa-1,3,5-trien-7-amine

: 1128112-41-3
3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

Guidance literature:: In N,N-dimethyl-formamide; at 160 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/anie.200804444

Reference yield: 68.0%

: 1128112-41-3
3-[2-(2-{[tert-buty(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-3,4-dihydroisoquinoline

: 3-[2-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-1,2,3,4-tetrahydroisoquinoline

: 3-[2-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)-4,5-dimethoxyphenyl]-6,7-dimethoxy-1-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1002/anie.200804444