2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

Base Information

• Chemical Name: 2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole
• CAS No.: 127945-34-0
• Molecular Formula: C₁₈H₂₂N₄O₄S
• Molecular Weight: 390.463

Synonyms:2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

Chemical Property of 2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

Chemical Property:

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Technology Process of 2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

There total 1 articles about 2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)pyrrole (38187-09-6) + Toluene-4-sulfonic acid (S)-2-phenyl-[1,3]dioxan-4-ylmethyl ester (72229-32-4,79413-94-8,95840-94-1,127945-31-7) → 2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole (127945-34-0)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMF, RT, 5 min, 2.) 100 deg C, 18 h;

DOI:10.1021/jm00170a019

Reference yield: 59.0%

2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole (127945-34-0) → 2-amino-3,4-dicyano-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole (127945-42-0)

Guidance literature:

With pyridine; p-toluenesulfonyl chloride; for 24h; Ambient temperature;

DOI:10.1021/jm00170a019

Reference yield: 54.0%

2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole (127945-34-0) → 2-amino-3,4-bis(aminocarbonyl)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole (127945-38-4)

Guidance literature:

With nickel; In ethanol; for 18h; Heating;

DOI:10.1021/jm00170a019

upstream raw materials:

2-amino-3,4-bis(aminocarbonyl)-5-(methylthio)pyrrole

Toluene-4-sulfonic acid (S)-2-phenyl-[1,3]dioxan-4-ylmethyl ester

Downstream raw materials:

2-amino-5-(aminocarbonyl)-6-(methylthio)-7-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrolo<2,3-d>pyrimidin-4-one

2-amino-3,4-bis(aminocarbonyl)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

2-amino-3,4-dicyano-5-(methylthio)-1-<(S)-2,4-O-benzylidene-2,4-dihydroxybutyl>pyrrole

2-amino-5-cyano-7-<(S)-2,4-dihydroxybutyl>pyrrolo<2,3-d>pyrimidin-4-one

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