3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene

Base Information

• Chemical Name: 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene
• CAS No.: 59945-65-2
• Molecular Formula: C₂₅H₂₉N₃O₅S₂
• Molecular Weight: 515.654

Synonyms:3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene

Chemical Property of 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene

There total 3 articles about 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1⁽¹⁵⁾,11,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.6%

2,6-bis-(bromomethyl)pyridine (7703-74-4) + N,N'-Bis(p-tolylsulfonyl)-1,5-diamino-3-oxapentane (59945-34-5) → 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1(15),11,13-triene (59945-65-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 22h; Reflux; Inert atmosphere;

Reference yield: 59.0%

2,6-bis(chloromethyl)pyridine (3099-28-3) + N,N'-Bis(p-tolylsulfonyl)-1,5-diamino-3-oxapentane (59945-34-5) → 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1(15),11,13-triene (59945-65-2)

Guidance literature:

With potassium carbonate; In acetonitrile; Molecular sieve; Inert atmosphere; Reflux;

DOI:10.3390/molecules27020371

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 3,9-bis((4-methylphenyl)sulfonyl)-6-oxa-3,9,15-triazabicyclo(9.3.1)entadeca-1(15),11,13-triene (59945-65-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water; diethyl ether / pH 12

2: potassium carbonate / acetonitrile / 22 h / Reflux; Inert atmosphere

With potassium carbonate; sodium hydroxide; In diethyl ether; water; acetonitrile;

upstream raw materials:

2,6-bis-(bromomethyl)pyridine

N,N'-Bis(p-tolylsulfonyl)-1,5-diamino-3-oxapentane

p-toluenesulfonyl chloride

2,6-bis(chloromethyl)pyridine

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