benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

Base Information

Chemical Name:benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate
CAS No.:184775-08-4
Molecular Formula:C₁₆H₁₆F₃NO₃
Molecular Weight:327.303
Hs Code.:

Synonyms:benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

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Chemical Property of benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

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Technology Process of benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

There total 3 articles about benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 40236-19-9
benzyl 3,5-dimethylpyrrole-2-carboxylate

: 433-27-2
ethyl trifluoroacetaldehyde hemiacetal

: 184775-08-4
benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

Guidance literature:: With zinc(II) chloride; In dichloromethane; for 28h; Ambient temperature;
DOI:10.1016/0040-4020(96)00858-7

Reference yield: 78.0%

: 75-90-1
2,2,2-Trifluoroacetaldehyde

: 40236-19-9
benzyl 3,5-dimethylpyrrole-2-carboxylate

: 184775-08-4
benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

Guidance literature:: With zinc(II) chloride;
DOI:10.1016/S0040-4020(01)00780-3

Reference yield: 78.0%

: 40236-19-9
benzyl 3,5-dimethylpyrrole-2-carboxylate

: 433-27-2
ethyl trifluoroacetaldehyde hemiacetal

: 184775-08-4
benzyl 4-(1-hydroxy-2,2,2-trifluoroethyl)-3,5-dimethylpyrrole-2-carboxylate

: C₃₀H₂₉F₃N₂O₄

Guidance literature:: With zinc(II) chloride; In dichloromethane; for 15h; Product distribution; Ambient temperature; var. Lewis acid, temp, and reaction time;
DOI:10.1016/0040-4020(96)00858-7