C₃₃H₃₄N₂O₇

Base Information

• Chemical Name: C₃₃H₃₄N₂O₇
• CAS No.: 1429512-52-6
• Molecular Formula: C₃₃H₃₄N₂O₇
• Molecular Weight: 570.642
• Mol file: 1429512-52-6.mol

Synonyms:C₃₃H₃₄N₂O₇

Chemical Property of C₃₃H₃₄N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₃₄N₂O₇

There total 4 articles about C₃₃H₃₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-(allyloxy)-4-oxobutanoic acid (3882-09-5) + C30H34N2O4 (1429512-59-3) → C33H34N2O7 (1429512-52-6)

Guidance literature:

4-(allyloxy)-4-oxobutanoic acid; C₃₀H₃₄N₂O₄; With 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide; In N,N-dimethyl-formamide;

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

Fmoc-Phe-H (146803-43-2) → C33H34N2O7 (1429512-52-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium cyanoborohydride; methanol

2: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide

3: trifluoroacetic acid / dichloromethane

With methanol; sodium cyanoborohydride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c2sc20428b

Reference yield:

C30H34N2O4 (1429512-59-3) → C33H34N2O7 (1429512-52-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 3-hydroxy-3,4-dihydrobenzotriazine-4-one; diisopropyl-carbodiimide / N,N-dimethyl-formamide

2: trifluoroacetic acid / dichloromethane

With 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c2sc20428b

upstream raw materials:

Fmoc-Phe-H

C₃₀H₃₄N₂O₄

4-(allyloxy)-4-oxobutanoic acid

Downstream raw materials:

C₈₄H₁₂₉N₁₅O₁₁

C₈₆H₁₃₃N₁₅O₁₁

C₁₀₃H₁₅₈N₁₈O₁₃

C₈₈H₁₃₇N₁₅O₁₁