C₄₉H₆₀N₈O₆

Base Information

Chemical Name:C₄₉H₆₀N₈O₆
CAS No.:1419385-74-2
Molecular Formula:C₄₉H₆₀N₈O₆
Molecular Weight:857.065
Hs Code.:

C<sub>49</sub>H<sub>60</sub>N<sub>8</sub>O<sub>6</sub>

Synonyms:C₄₉H₆₀N₈O₆

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Chemical Property of C₄₉H₆₀N₈O₆

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Technology Process of C₄₉H₆₀N₈O₆

There total 14 articles about C₄₉H₆₀N₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.8%

: C₃₅H₃₈N₆*4ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1419385-74-2
C₄₉H₆₀N₈O₆

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 10h;

Reference yield:

: 1419387-60-2
C₁₅H₁₈O₂

: 1419385-74-2
C₄₉H₆₀N₈O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

3.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

3.2: 4 h / 0 °C

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 1 h / 20 °C / Cooling with ice

5.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C / Sealed tube

6.1: hydrogenchloride / ethyl acetate / 20 °C

7.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 0 - 20 °C

With pyridine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; ammonium acetate; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: 1419391-59-5
C₄₅H₅₄N₂O₁₀

: 1419385-74-2
C₄₉H₆₀N₈O₆

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C / Sealed tube

2: hydrogenchloride / ethyl acetate / 20 °C

3: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 0 - 20 °C

With hydrogenchloride; ammonium acetate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; ethyl acetate;