6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

Base Information

Chemical Name:6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en
CAS No.:140676-45-5
Molecular Formula:C₄₉H₅₂N₄O₆S₂
Molecular Weight:857.107
Hs Code.:

Synonyms:6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

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Chemical Property of 6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

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Technology Process of 6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

There total 6 articles about 6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 140661-52-5
Bis<4-(5-iodpentyl)phenyl>methan

: 140661-33-2
3,3'-Bis<(4-methoxyphenylsulfonyl)amino>azobenzol

: 140676-45-5
6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 12h;

Reference yield:

: 21371-44-8,140661-36-5
3,3'-diaminoazobenzene

: 140676-45-5
6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 2 h / 70 °C

2: 43 percent / Cs₂CO₃ / dimethylformamide / 12 h / 60 °C

With pyridine; caesium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 102887-52-5
5,5'-(4,4'-methanediyl-di-phenyl)-di-valeric acid

: 140676-45-5
6,21-Bis(4-methoxyphenylsulfonyl)-6,13,14,21-tetraaza<6.2.6.1>(1,3)(1,3)(1,4)(1,4)cyclophan-13-en

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, DMF / 3 h / Heating

2: 88 percent / LiAlH₄ / tetrahydrofuran / a) 4 h, reflux, b) 12 h, r.t.

3: 72 percent / 57percent HI / 10 h / Heating

4: 43 percent / Cs₂CO₃ / dimethylformamide / 12 h / 60 °C

With lithium aluminium tetrahydride; thionyl chloride; hydrogen iodide; caesium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; N,N-dimethyl-formamide;