4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran

Base Information

• Chemical Name: 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran
• CAS No.: 136617-95-3
• Molecular Formula: C₂₆H₄₂O₃Si
• Molecular Weight: 430.703

Synonyms:4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran

Chemical Property of 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran

Chemical Property:

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Technology Process of 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran

There total 4 articles about 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[1-hydroxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran → 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran (136617-95-3)

Guidance literature:

With pyridine; acetic anhydride;

Reference yield:

2-(trimethylsilyl)-4-furaldehyde (105426-88-8) → 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran (136617-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 2.) 0 deg C, THF

2: tetrahydrofuran / Ambient temperature

With magnesium; In tetrahydrofuran;

DOI:10.1021/jo00025a012

Reference yield:

2-((E)-6-Bromo-3-methyl-hex-3-enyl)-1,3,3-trimethyl-cyclohexene (120756-54-9) → 4-[1-acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)-hept-4-ene]-2-trimethylsilylfuran (136617-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 2.) 0 deg C, THF

2: tetrahydrofuran / Ambient temperature

With magnesium; In tetrahydrofuran;

DOI:10.1021/jo00025a012

upstream raw materials:

acetic anhydride

2-(trimethylsilyl)-4-furaldehyde

2-((E)-6-Bromo-3-methyl-hex-3-enyl)-1,3,3-trimethyl-cyclohexene

Downstream raw materials:

4-[1-Acetoxy-5-methyl-7-(2,6,6-trimethylcyclohex-1-enyl)hept-4-ene]-5-hydroxy-2(5H)-furanone

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