C₂₁H₂₉NO₆S

Base Information

Chemical Name:C₂₁H₂₉NO₆S
CAS No.:1393086-03-7
Molecular Formula:C₂₁H₂₉NO₆S
Molecular Weight:423.53
Hs Code.:

C<sub>21</sub>H<sub>29</sub>NO<sub>6</sub>S

Synonyms:C₂₁H₂₉NO₆S

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Chemical Property of C₂₁H₂₉NO₆S

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Technology Process of C₂₁H₂₉NO₆S

There total 5 articles about C₂₁H₂₉NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1234286-97-5
ethyl 3,4-O-isopentylidene-5α-amino shikimate

: 98-59-9
p-toluenesulfonyl chloride

: 1393086-03-7
C₂₁H₂₉NO₆S

Guidance literature:: With pyridine; dmap; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2012.06.065

Reference yield:

: 1234286-95-3
ethyl 3,4-O-isopentylidene-5-oxo shikimate

: 1393086-03-7
C₂₁H₂₉NO₆S

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate; molybdenum(VI) oxide / methanol / 0.5 h / 20 °C / Inert atmosphere

3: pyridine; dmap / 12 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; hydroxylamine hydrochloride; molybdenum(VI) oxide; In methanol; ethanol;
DOI:10.1016/j.tet.2012.06.065

Reference yield:

: 1393086-01-5
C₂₅H₃₇O₉P

: 1393086-03-7
C₂₁H₂₉NO₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 5%-palladium/activated carbon; hydrogen / ethanol / 120 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0.75 h / 20 °C / Inert atmosphere; Cooling

4.1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate; molybdenum(VI) oxide / methanol / 0.5 h / 20 °C / Inert atmosphere

6.1: pyridine; dmap / 12 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; 5%-palladium/activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydride; molybdenum(VI) oxide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.065