methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside

Base Information

• Chemical Name: methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside
• CAS No.: 133934-05-1
• Molecular Formula: C₁₅H₁₇F₃O₇S
• Molecular Weight: 398.357

Synonyms:methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside

Chemical Property of methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside

There total 2 articles about methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-ribo-hexopyranoside (133934-01-7) → methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside (133934-05-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / tetrabutylammonium nitrite / toluene / 48 h / 23 °C

2: pyridine / CH₂Cl₂ / 0.5 h / -20 deg C to r.t.

With pyridine; tetrabutylammonium nitrite; In dichloromethane; toluene;

DOI:10.1021/jo00012a020

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + methyl 3-O-benzoyl-2,6-dideoxy-β-D-xylo-hexopyranoside (133933-99-0) → methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside (133934-05-1)

Guidance literature:

With pyridine; In dichloromethane; for 0.5h; -20 deg C to r.t.;

DOI:10.1021/jo00012a020

Reference yield: 100.0%

methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-xylo-hexopyranoside (133934-05-1) → methyl 3-O-benzoyl-2,6-dideoxy-β-D-ribo-hexopyranoside (102650-57-7)

Guidance literature:

With water; In pyridine; dichloromethane; for 96h; Ambient temperature;

DOI:10.1021/jo00012a020

upstream raw materials:

trifluoromethylsulfonic anhydride

methyl 3-O-benzoyl-2,6-dideoxy-β-D-xylo-hexopyranoside

methyl 3-O-benzoyl-2,6-dideoxy-4-O-<(trifluoromethyl)sulfonyl>-β-D-ribo-hexopyranoside

Downstream raw materials:

methyl 3-O-benzoyl-2,6-dideoxy-β-D-ribo-hexopyranoside

methyl 4-O-benzoyl-2,6-dideoxy-β-D-ribo-hexopyranoside

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