C₇₃H₈₄N₄O₁₃SiZn

Base Information

Chemical Name:C₇₃H₈₄N₄O₁₃SiZn
CAS No.:1033224-35-9
Molecular Formula:C₇₃H₈₄N₄O₁₃SiZn
Molecular Weight:1318.96
Hs Code.:

C<sub>73</sub>H<sub>84</sub>N<sub>4</sub>O<sub>13</sub>SiZn

Synonyms:C₇₃H₈₄N₄O₁₃SiZn

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Chemical Property of C₇₃H₈₄N₄O₁₃SiZn

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Technology Process of C₇₃H₈₄N₄O₁₃SiZn

There total 2 articles about C₇₃H₈₄N₄O₁₃SiZn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: tetraethyl 4,4',4'',4'''-[(10-{5-hydroxy-2-[(triisopropylsilyl)ethynyl]phenyl}porphyrin-5,15-diyl)bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate

: 1033224-35-9
C₇₃H₈₄N₄O₁₃SiZn

Guidance literature:: With zinc(II) acetate dihydrate; In methanol; chloroform; at 65 ℃; for 1h;
DOI:10.1002/chem.200802077

Reference yield: 96.0%

: ((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(HO)C₆H₃)C₂₀H₁₁N₄

: 5970-45-6
zinc(II) acetate dihydrate

: 1033224-35-9
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(HO)C₆H₃)C₂₀H₉N₄)Zn

Guidance literature:: In methanol; chloroform; reaction of porphyrin deriv. with zinc compd. in CHCl3/methanol at 65.dgree.C for 1 h;
DOI:10.1002/anie.200705180

Reference yield: 79.0%

: 1033224-35-9
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(HO)C₆H₃)C₂₀H₉N₄)Zn

: 126311-74-8
1-(6-bromohexyl)-1H-imidazole

: 1033224-37-1
(((CH₃CH₂OOCCH₂CH₂CH₂O)2C₆H₃)2(((CH₃)2CH)3SiCC(C₃H₃N₂(CH₂)6O)C₆H₃)C₂₀H₉N₄)Zn

Guidance literature:: With Cs₂CO₃; In N,N-dimethyl-formamide; treatment of porphyrin deriv. with imidazole deriv. in DMF in presence of Cs2CO3 at 20°C for 14 h;
DOI:10.1002/anie.200705180