benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

Base Information

Chemical Name:benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside
CAS No.:174151-36-1
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

Synonyms:benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

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Chemical Property of benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

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Technology Process of benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

There total 8 articles about benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131085-43-3
benzyl 2-benzyloxycarbonylamino-2,3,4,6-tetradeoxy-α-D-erythro-hex-3-enopyranoside

: 174151-36-1
benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1016/0008-6215(95)00291-X

Reference yield:

: Methanesulfonic acid (2S,3R,4R,5R,6R)-2-benzyloxy-3-benzyloxycarbonylamino-5-hydroxy-6-methyl-tetrahydro-pyran-4-yl ester

: 174151-36-1
benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; Yield given;
DOI:10.1016/0008-6215(95)00291-X

Reference yield:

: 2864-17-7
benzyl O⁴,O⁶-(R)-benzylidene-2-benzyloxycarbonylamino-O³-methanesulfonyl-α-D-2-deoxy-glucopyranoside

: 174151-36-1
benzyl 3,4-anhydro-2-benzyloxycarbonylamino-2,6-dideoxy-α-D-alloppyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / BaCO₃, NBS / CCl₄; various solvent(s) / 2 h / Heating

2: 84 percent / tributyltin hydride, α,α'-azobisisobutyronitrile / benzene / 3 h / Heating

3: K₂CO₃ / methanol / 4 h / Ambient temperature

4: NaH / tetrahydrofuran

With N-Bromosuccinimide; azobisisobutyronitrile; tri-n-butyl-tin hydride; sodium hydride; potassium carbonate; barium carbonate; In tetrahydrofuran; methanol; tetrachloromethane; benzene;
DOI:10.1016/0008-6215(95)00291-X