5,7,8,15-Tetrahydro-2,3-dimethoxy-6-methylbenzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one

Base Information

Chemical Name:5,7,8,15-Tetrahydro-2,3-dimethoxy-6-methylbenzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one
CAS No.:528-67-6
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:
Mol file:528-67-6.mol

Synonyms:Benzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one,5,7,8,15-tetrahydro-2,3-dimethoxy-6-methyl- (7CI,8CI); Fagarine II (6CI);[1,3]Benzodioxolo[5,6-e][2]benzazecin-14(6H)-one,5,7,8,15-tetrahydro-2,3-dimethoxy-6-methyl- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,7,8,15-Tetrahydro-2,3-dimethoxy-6-methylbenzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one

Chemical Property:

PSA：57.23000
LogP:2.78370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5,7,8,15-Tetrahydro-2,3-dimethoxy-6-methylbenzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one

There total 10 articles about 5,7,8,15-Tetrahydro-2,3-dimethoxy-6-methylbenzo[e][1,3]dioxolo[4,5-k][3]benzazecin-14(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 74059-78-2
2,3-Dimethoxy-6-methyl-5,6,7,8,14,15-hexahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-g]azecin-14-ol

: 528-67-6
Fagarin II

Guidance literature:: With manganese(IV) oxide; In chloroform; for 1h; Ambient temperature;

Reference yield:

: 4078-66-4
(14E)-2,3-dimethoxy-6-methyl-5,6,7,8-tetrahydro-benzo[c][1,3]dioxolo[4',5':4,5]benzo[1,2-g]azecine 6-oxide

: 528-67-6
Fagarin II

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1016/S0040-4020(01)98521-7

Reference yield:

: 6656-19-5,28319-56-4
(+-)-2,3-methylenedioxy-10,11-dimethoxy-5,8,13,13a-tetrahydro-6H-dibenzo[a,g]quinolizine

: 528-67-6
Fagarin II

Guidance literature:: Multi-step reaction with 3 steps

1: (i), (ii) Ag₂O

2: (PhCO)2O₂

3: aq. HCl / acetic acid

With hydrogenchloride; dibenzoyl peroxide; In acetic acid;
DOI:10.1016/S0040-4020(01)98521-7