4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride

Base Information

• Chemical Name: 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride
• CAS No.: 947689-89-6
• Molecular Formula: C₁₅H₁₁ClN₄O₄S
• Molecular Weight: 378.796

Synonyms:4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride

Chemical Property of 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride

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Technology Process of 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride

There total 1 articles about 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-(6-{3-[4-(benzylthio)phenyl]-1,2,4-oxadiazol-5-yl}pyridin-2-yl)acetamide (947689-77-2) → 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride (947689-89-6)

Guidance literature:

With water; chlorine; acetic acid; at 5 - 10 ℃; for 0.25h;

Reference yield: 24.0%

N-(3-Amino-5-fluorophenyl)-1-cyanocyclopropanecarboxamide (947689-80-7) + 4-[5-(6-acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]benzenesulfonylchloride (947689-89-6) → N-{3-[({4-[5-(6-Acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]phenyl}sulfonyl)amino]-5-fluorophenyl}-1-cyanocyclopropanecarboxamide (947689-94-3)

Guidance literature:

With pyridine; at 20 ℃; for 18h;

upstream raw materials:

N-(6-{3-[4-(benzylthio)phenyl]-1,2,4-oxadiazol-5-yl}pyridin-2-yl)acetamide

Downstream raw materials:

N-{3-[({4-[5-(6-Acetylaminopyridin-2-yl)-1,2,4-oxadiazol-3-yl]phenyl}sulfonyl)amino]-5-fluorophenyl}-1-cyanocyclopropanecarboxamide

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