N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

Base Information

Chemical Name:N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride
CAS No.:951646-66-5
Molecular Formula:C₁₅H₁₉F₃N₂O₂S*ClH
Molecular Weight:384.85
Hs Code.:

Synonyms:N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

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Chemical Property of N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

Chemical Property:

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Technology Process of N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

There total 3 articles about N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 951646-76-7
3-[N-cyclopropyl-N-(3-trifluoromethylbenzenesulfonyl)amino]piperidine-1-carboxylic acid tert-butyl ester

: 951646-66-5
N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; at 20 ℃; for 48h;

Reference yield:

: 887588-04-7,1354008-67-5
3-(cyclopropylamino)piperidine-1-carboxylic acid tert-butyl ester

: 951646-66-5
N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 48 h / 20 - 37 °C

2: hydrogenchloride; water / 1,4-dioxane / 48 h / 20 °C

With hydrogenchloride; water; triethylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: 98977-36-7
3-oxo-piperidine-1-carboxylic acid tert-butyl ester

: 951646-66-5
N-cyclopropyl-N-piperidin-3-yl-3-trifluoromethylbenzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 24 h / 0 - 20 °C / Molecular sieve

2: triethylamine / dichloromethane / 48 h / 20 - 37 °C

3: hydrogenchloride; water / 1,4-dioxane / 48 h / 20 °C

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; triethylamine; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;