6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

Base Information

Chemical Name:6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene
CAS No.:119273-70-0
Molecular Formula:C₃₉H₂₆Br₂O₂
Molecular Weight:686.442
Hs Code.:

Synonyms:6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

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Chemical Property of 6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

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Technology Process of 6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

There total 3 articles about 6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 106750-88-3
6,7-dibromo-1,4-epoxy-1,4-dihydronaphthalene

: 479-33-4
2,3,4,5-tetraphenylcyclopenta-2,4-dienone

: 119273-70-0
6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

Guidance literature:: In benzene; for 48h; Heating;
DOI:10.1021/jo00268a053

Reference yield:

: 636-28-2
1,2,4,5-tetrabromobenzene

: 119273-70-0
6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / hexane; toluene / -20 - 20 °C / Inert atmosphere

2: ethanol / 36 h / Reflux

With n-butyllithium; In ethanol; hexane; toluene;
DOI:10.1002/chem.201100443

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 119273-70-0
6,7-dibromo-1,4-carbonylo-9,10-epoxy-1,2,3,4-tetraphenyl-1,4,4a,9,9a,10-hexahydroanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: iron(III) chloride; bromine / chloroform / 0 - 45 °C

2: n-butyllithium / hexane; toluene / -20 - 20 °C / Inert atmosphere

3: ethanol / 36 h / Reflux

With iron(III) chloride; n-butyllithium; bromine; In ethanol; hexane; chloroform; toluene;
DOI:10.1002/chem.201100443