Technology Process of C15H13N3O2S
There total 3 articles about C15H13N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / dichloromethane / 0 - 20 °C
2: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 100 °C
3: palladium 10% on activated carbon / toluene / 100 °C / Sealed tube
With
N-Bromosuccinimide; palladium 10% on activated carbon; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
dichloromethane; toluene;
2: |Buchwald-Hartwig Coupling;
DOI:10.2174/1570178611310040002
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 100 °C
2: palladium 10% on activated carbon / toluene / 100 °C / Sealed tube
With
palladium 10% on activated carbon; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
In
toluene;
1: |Buchwald-Hartwig Coupling;
DOI:10.2174/1570178611310040002