2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl

Base Information

• Chemical Name: 2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl
• CAS No.: 128445-71-6
• Molecular Formula: C₂₈H₂₉N₃O*ClH
• Molecular Weight: 460.019

Synonyms:2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl

Chemical Property of 2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl

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Technology Process of 2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl

There total 1 articles about 2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

8-Butyl-12-[1-phenyl-meth-(E)-ylidene]-6,7,9,10,11,12-hexahydro-1,3,13,14-tetraaza-pentaphene (114301-20-1) → 2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl (128445-71-6)

Guidance literature:

With hydrogenchloride; Heating;

Reference yield: 91.0%

2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl (128445-71-6) + malononitrile (109-77-3) → 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline (157226-31-8)

Guidance literature:

With piperidine; In ethanol; for 6h; Heating;

DOI:10.1016/0040-4020(94)00902-7

Reference yield: 88.0%

2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl (128445-71-6) + ethyl 2-cyanoacetate (105-56-6) → 12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline-2(1H)-one

Guidance literature:

With piperidine; In ethanol; for 6h; Heating;

DOI:10.1016/0040-4020(94)00902-7

upstream raw materials:

8-Butyl-12-[1-phenyl-meth-(E)-ylidene]-6,7,9,10,11,12-hexahydro-1,3,13,14-tetraaza-pentaphene

Downstream raw materials:

2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline

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