2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI)

Base Information

• Chemical Name: 2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI)
• CAS No.: 730907-52-5
• Molecular Formula: C₁₃H₁₇NO₂
• Molecular Weight: 219.283
• Mol file: 730907-52-5.mol

Synonyms:2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI)

Chemical Property of 2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI)

Chemical Property:

• PSA: 29.54000
• LogP: 2.74380

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI)

There total 4 articles about 2-Oxazolidinone,4-ethyl-5-methyl-3-(phenylmethyl)-,(4R,5S)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl-(1-ethyl-2-phenylselanyl-propyl)-carbamic acid tert-butyl ester → cis-3-benzyl-4-ethyl-5-methyl-oxazolidin-2-one (730907-52-5) + trans-3-benzyl-4-ethyl-5-methyl-oxazolidin-2-one (730907-52-5)

Guidance literature:

benzyl-(1-ethyl-2-phenylselanyl-propyl)-carbamic acid tert-butyl ester; With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 0.333333h;

With sodium carbonate; In acetonitrile; Title compound not separated from byproducts;

DOI:10.1039/b406566m

Reference yield:

benzyl-(1-ethyl-2-phenylselanyl-propyl)-carbamic acid tert-butyl ester → cis-3-benzyl-4-ethyl-5-methyl-oxazolidin-2-one (730907-52-5) + trans-3-benzyl-4-ethyl-5-methyl-oxazolidin-2-one (730907-52-5)

Guidance literature:

benzyl-(1-ethyl-2-phenylselanyl-propyl)-carbamic acid tert-butyl ester; With N-Bromosuccinimide; In acetonitrile; at 20 ℃; for 0.333333h;

With sodium carbonate; In acetonitrile; Title compound not separated from byproducts;

DOI:10.1039/b406566m

Reference yield:

N-benzyl-2-(phenylselanyl)pentan-3-amine → cis-3-benzyl-4-ethyl-5-methyl-oxazolidin-2-one (730907-52-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-bromosuccinimide / acetonitrile / 0.33 h / 20 °C

1.2: Na₂CO₃ / acetonitrile

With N-Bromosuccinimide; In acetonitrile;

DOI:10.1039/b406566m

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