2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Base Information

Chemical Name:2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate
CAS No.:1031364-59-6
Molecular Formula:C₅₁H₇₃NO₁₉
Molecular Weight:1004.14
Hs Code.:

2,7-(OMHEG)2-2'-(CH<sub>2</sub>OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Synonyms:2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

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Chemical Property of 2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

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Technology Process of 2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

There total 9 articles about 2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1031364-12-1
methyl 3-methoxymethyl-4-hydroxy-5-methylbenzoate

: 1031364-52-9
2,7-(OMHEG)2-acridine-9-carboxylic acid

: 1031364-59-6
2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: 2,7-(OMHEG)2-acridine-9-carboxylic acid; With pyridine; p-toluenesulfonyl chloride; at 20 ℃; for 0.0833333h; Inert atmosphere;

methyl 3-methoxymethyl-4-hydroxy-5-methylbenzoate; at 20 ℃; for 120h;

Reference yield:

: 172834-75-2
2,7-dimethoxy acridine-9-carboxylic acid

: 1031364-59-6
2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 1 h / Reflux; Inert atmosphere

2.1: pyridine / 37 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 48 h / 20 °C

3.2: 20 °C / Cooling with ice

4.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

5.1: potassium hydroxide; water / 16 h / 20 °C

6.1: pyridine; p-toluenesulfonyl chloride / 0.08 h / 20 °C / Inert atmosphere

6.2: 120 h / 20 °C

With pyridine; thionyl chloride; water; boron tribromide; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1031364-44-9
C₁₇H₁₅NO₄

: 1031364-59-6
2,7-(OMHEG)2-2'-(CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / 48 h / 20 °C

1.2: 20 °C / Cooling with ice

2.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

3.1: potassium hydroxide; water / 16 h / 20 °C

4.1: pyridine; p-toluenesulfonyl chloride / 0.08 h / 20 °C / Inert atmosphere

4.2: 120 h / 20 °C

With pyridine; water; boron tribromide; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;