9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole

Base Information

• Chemical Name: 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole
• CAS No.: 1185197-60-7
• Molecular Formula: C₅₆H₇₁NOS₃
• Molecular Weight: 870.384

Synonyms:9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole

Chemical Property of 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole

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Technology Process of 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole

There total 1 articles about 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5,5-dimethyl-2-(4-n-hexylthiophen-2-yl)-1,3,2-dioxaborinane (1060683-81-9) + 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(5'-bromo-3,4'-di-n-hexyl-[2,2']bithiophen-5-yl)-9H-carbazole (1185197-58-3) → 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole (1185197-60-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; Reflux;

DOI:10.1039/b905831a

Reference yield: 92.0%

9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole (1185197-60-7) → 9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(5''-bromo-3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole (1185197-62-9)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b905831a

Reference yield: 64.0%

9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole (1185197-60-7) → 5''-[9-ethyl-3-(4-(n-hexyloxy)phenyl)-9H-carbazol-6-yl]-3',3'',4-tri-n-hexyl-[2,2',5',2'']terthiophene-5-carbalehyde (1185197-61-8)

Guidance literature:

With N,N-dimethyl-formamide; trichlorophosphate; at 0 - 70 ℃;

DOI:10.1039/b905831a

upstream raw materials:

5,5-dimethyl-2-(4-n-hexylthiophen-2-yl)-1,3,2-dioxaborinane

9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(5'-bromo-3,4'-di-n-hexyl-[2,2']bithiophen-5-yl)-9H-carbazole

Downstream raw materials:

5''-[9-ethyl-3-(4-(n-hexyloxy)phenyl)-9H-carbazol-6-yl]-3',3'',4-tri-n-hexyl-[2,2',5',2'']terthiophene-5-carbalehyde

9-ethyl-3-(4-(n-hexyloxy)phenyl)-6-(5''-bromo-3,4',4''-tri-n-hexyl-[2,2',5',2'']terthiophen-5-yl)-9H-carbazole

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