allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Base Information

• Chemical Name: allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate
• CAS No.: 524072-17-1
• Molecular Formula: C₃₁H₄₉NO₅Si₂
• Molecular Weight: 571.905

Synonyms:allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Chemical Property of allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Chemical Property:

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Safty Information:

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Technology Process of allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

There total 1 articles about allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl ((3S,4R)-2-oxo-4-[2-oxo-2-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-ethyl]-3-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-azetidin-1-yl) (triphenylphosphoranilidene) acetate (524072-16-0) → allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-17-1)

Guidance literature:

In toluene; at 130 ℃; for 2.5h;

Reference yield:

allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-17-1) → allyl (5R,6S)-3-[3-(hydroxymethyl)-phenyl]-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-19-3)

Guidance literature:

With acetic acid; In tetrahydrofuran; water; at 0 ℃; for 0.5h;

Reference yield:

allyl (5R,6S)-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-3-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-17-1) + trifluorormethanesulfonic acid (1493-13-6) → allyl (5R,6S)-6-[(1R)-1-hydroxyethyl]-3-[3-(hydroxymethyl)-phenyl]-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-18-2)

Guidance literature:

In tetrahydrofuran; water; at 0 ℃; for 1h; pH=2.2;

upstream raw materials:

allyl ((3S,4R)-2-oxo-4-[2-oxo-2-(3-{[(triethylsilyl)-oxy]-methyl}-phenyl)-ethyl]-3-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-azetidin-1-yl) (triphenylphosphoranilidene) acetate

Downstream raw materials:

allyl (5R,6S)-6-[(1R)-1-hydroxyethyl]-3-[3-(hydroxymethyl)-phenyl]-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

allyl (5R,6S)-3-[3-(hydroxymethyl)-phenyl]-7-oxo-6-{(1R)-1-[(triethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

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