1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

Base Information

Chemical Name:1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane
CAS No.:175469-04-2
Molecular Formula:C₄₀H₄₆O₁₂
Molecular Weight:718.798
Hs Code.:

Synonyms:1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

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Technology Process of 1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

There total 1 articles about 1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40101-08-4
1,2-bis(2,3-dimethoxyphenyl)ethane

: 175469-04-2
1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) nBuLi, TMEDA / 1.) Et₂O, hexane, 3 h, 2.) Et₂O, hexane, 4 h

2: 100 percent / 3 h / Heating

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
DOI:10.1016/0040-4020(95)01064-5

Reference yield: 91.0%

: 175469-04-2
1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

: 175469-05-3
1,2-bis(4-(2,3-dimethoxybenzyl) 2,3-dimethoxyphenyl)ethane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; for 15h; under 33752.7 Torr;
DOI:10.1016/0040-4020(95)01064-5

Reference yield:

: 175469-04-2
1,2-bis(4-((2,3-dimethoxyphenyl)acetoxymethyl) 2,3-dimethoxyphenyl)ethane

: 1,2-bis(4-(2,3-dihydroxybenzyl) 2,3-dihydroxyphenyl)ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / H₂ / Pd/C / ethyl acetate; methanol / 15 h / 33752.7 Torr

2: 72 percent / BBr₃ / CH₂Cl₂ / 18 h / 0 - 20 °C

With hydrogen; boron tribromide; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1016/0040-4020(95)01064-5