3-Phenyl-4-formylsydnone

Base Information

Chemical Name:3-Phenyl-4-formylsydnone
CAS No.:14484-83-4
Molecular Formula:C₉H₆N₂O₃
Molecular Weight:190.158
Hs Code.:
DSSTox Substance ID:DTXSID301186399

Synonyms:3-phenyl-4-formylsydnone;14484-83-4;SCHEMBL7378883;DTXSID301186399;AKOS005214202;1,2,3-Oxadiazolium, 4-formyl-5-hydroxy-3-phenyl-, inner salt

Suppliers and Price of 3-Phenyl-4-formylsydnone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Phenyl-4-formylsydnone

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:190.03784206
Heavy Atom Count:14
Complexity:206

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[N+]2=NOC(=C2C=O)[O-]

Technology Process of 3-Phenyl-4-formylsydnone

There total 8 articles about 3-Phenyl-4-formylsydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 4-(hydroxymethyl)-3-phenyl-1,2,3-oxadiazol-3-ium-5-olate

: 14484-83-4
4-formyl-3-phenyl-sydnone

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo400381a

Reference yield: 53.0%

: 508191-77-3
3-phenylsydnone

: 93-61-8
N-methyl-N-phenylformamide

: 14484-83-4
4-formyl-3-phenyl-sydnone

Guidance literature:: N-methyl-N-phenylformamide; With trichlorophosphate; for 0.5h;

3-phenylsydnone; at 45 ℃;

With water; In acetone;
DOI:10.1016/j.ejmech.2012.06.011

Reference yield:

: 103-01-5
N-Phenylglycine

: 14484-83-4
4-formyl-3-phenyl-sydnone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 2.5 h / 0 °C

2.1: acetic anhydride / Heating

3.1: trichlorophosphate / 0.5 h

3.2: 45 °C

With hydrogenchloride; acetic anhydride; sodium nitrite; trichlorophosphate; In water;
DOI:10.1016/j.ejmech.2012.06.011