benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate

Base Information

• Chemical Name: benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate
• CAS No.: 1579276-22-4
• Molecular Formula: C₂₇H₄₅N₃O₈
• Molecular Weight: 539.67

Synonyms:benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate

Chemical Property of benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate

Chemical Property:

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Technology Process of benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate

There total 1 articles about benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

glycine benzyl ester p-toluenesulfonic acid salt (1738-76-7) + methanesulfonic acid 2-(2-tert-butoxycarbonylamino-ethoxy)-ethyl ester (302331-20-0) → benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate (1579276-22-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; triethylamine; In 1,4-dioxane; at 90 ℃; for 24h;

Reference yield: 80.0%

benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate (1579276-22-4) + toluene-4-sulfonic acid (104-15-4) → benzyl 2-(bis(2-(2-aminoethoxy)ethyl)amino)acetate tri(p-toluenesulfonate)

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 0.5h;

DOI:10.1002/cmdc.201600270

Reference yield: 79.0%

benzyl 2-[bis[2-[2-(tert-butoxycarbonylamino)ethoxy]ethyl]amino]acetate (1579276-22-4) + toluene-4-sulfonic acid (104-15-4) → benzyl 2-(bis(2-(2-aminoethoxy)ethyl)amino)acetate tri(p-toluenesulfonate)

Guidance literature:

With water; In tetrahydrofuran; water; at 50 ℃; for 0.5h;

upstream raw materials:

glycine benzyl ester p-toluenesulfonic acid salt

methanesulfonic acid 2-(2-tert-butoxycarbonylamino-ethoxy)-ethyl ester

Downstream raw materials:

C₅₇H₁₀₃N₉O₁₈

benzyl 2-[bis[2-[2-(3-carboxypropanamido)ethoxy]ethyl]amino]acetate triethylammonium

C₄₇H₈₅N₇O₁₆

C₄₁H₆₉N₃O₁₂

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