6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

Base Information

Chemical Name:6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran
CAS No.:112183-05-8
Molecular Formula:C₁₈H₁₃F₃O₅S₂
Molecular Weight:430.425
Hs Code.:

Synonyms:6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

Suppliers and Price of 6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

There total 2 articles about 6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 112183-09-2
6-hydroxy-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-1-benzopyran

: 112183-05-8
6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(00)95932-X

Reference yield:

: 112183-10-5
2-(phenylthio)-5-(trimethylsilyl)-4-pentyn-1-ol

: 112183-05-8
6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

Guidance literature:: Multi-step reaction with 2 steps

2: 93 percent / Et₃N / CH₂Cl₂ / 0.17 h / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95932-X

Reference yield: 90.0%

: 112183-05-8
6-<(trifluoromethyl)sulfonyl>-3-(phenylthio)-(2,3,4H)-furo<2,3-h>-benzopyran

: 112183-08-1
3-(phenylthio)-(2,3,4H)-furo<2,3-h>-1-benzopyran

Guidance literature:: With formic acid; tributyl-amine; bis(acetato)bis(triphenylphosphine)palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 70 ℃; for 2.5h;
DOI:10.1016/S0040-4039(00)95932-X