C₅₉H₆₄N₄O₁₄

Base Information

Chemical Name:C₅₉H₆₄N₄O₁₄
CAS No.:1415996-41-6
Molecular Formula:C₅₉H₆₄N₄O₁₄
Molecular Weight:1053.18
Hs Code.:

C<sub>59</sub>H<sub>64</sub>N<sub>4</sub>O<sub>14</sub>

Synonyms:C₅₉H₆₄N₄O₁₄

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Chemical Property of C₅₉H₆₄N₄O₁₄

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Technology Process of C₅₉H₆₄N₄O₁₄

There total 14 articles about C₅₉H₆₄N₄O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1415996-66-5
C₆₁H₆₅ClN₄O₁₅

: 1415996-41-6
C₅₉H₆₄N₄O₁₄

Guidance literature:: With 2,6-dimethylpyridine; thiourea; In N,N-dimethyl-formamide; at 50 ℃; for 12h;
DOI:10.1039/c2ob26928g

Reference yield:

: 460082-41-1
phenyl 2-O-benzoyl-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 1415996-41-6
C₅₉H₆₄N₄O₁₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 5 h / -10 °C / Molecular sieve; Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane; methanol / 0.5 h / 0 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h / 0 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

5.1: 1,1'-sulfinylbisbenzene; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / -60 - -40 °C / Molecular sieve; Inert atmosphere

5.2: -60 - 20 °C / Inert atmosphere

6.1: thiourea; 2,6-dimethylpyridine / N,N-dimethyl-formamide / 12 h / 50 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; [bis(acetoxy)iodo]benzene; 1,1'-sulfinylbisbenzene; potassium carbonate; thiourea; trifluoroacetic acid; 2,4,6-tri-tert-butylpyrimidine; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26928g

Reference yield:

: 183875-35-6
phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-azido-1-thiol-α-D-glucopyranoside

: 1415996-41-6
C₅₉H₆₄N₄O₁₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium methylate / methanol / 5 h / 20 °C

2.1: trimethyl orthoformate; camphor-10-sulfonic acid / N,N-dimethyl-formamide / 36 h / 70 °C

3.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

4.1: trimethylamine-borane; aluminum (III) chloride / tetrahydrofuran / 24 h / 20 °C / Molecular sieve

5.1: pyridine / dichloromethane / 0 - 20 °C

6.1: N-Bromosuccinimide; water / acetone / 6 h / 0 °C

7.1: 1,1'-sulfinylbisbenzene; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / -60 - -40 °C / Molecular sieve; Inert atmosphere

7.2: -60 - 20 °C / Inert atmosphere

8.1: thiourea; 2,6-dimethylpyridine / N,N-dimethyl-formamide / 12 h / 50 °C

With pyridine; 2,6-dimethylpyridine; aluminum (III) chloride; N-Bromosuccinimide; trifluoromethylsulfonic anhydride; trimethylamine-borane; 1,1'-sulfinylbisbenzene; camphor-10-sulfonic acid; water; sodium methylate; sodium hydride; thiourea; 2,4,6-tri-tert-butylpyrimidine; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c2ob26928g