(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

Base Information

Chemical Name:(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide
CAS No.:118673-35-1
Molecular Formula:C₁₇H₂₀N₂O₆S
Molecular Weight:380.422
Hs Code.:

Synonyms:(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

Chemical Property:

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Technology Process of (1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

There total 3 articles about (1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: (1S,3S,5R,6R)-3-diazoacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

: 118673-35-1
(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

Guidance literature:: With sulfuric acid; In 1,4-dioxane; for 24h;

Reference yield:

: 15583-33-2
(3S,5R,6R)-3-diazoacetyl-2,2-dimethyl-6-phenoxyacetamidopenam

: 118673-35-1
(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium periodate / H₂O; methanol / 18 h

2: 44 percent / 3M sulphuric acid / dioxane / 24 h

With sodium periodate; sulfuric acid; In 1,4-dioxane; methanol; water;

Reference yield:

: 132-98-9
penicillin V potassium

: 118673-35-1
(1S,3S,5R,6R)-3-hydroxyacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine hydrochloride, ethyl chloroformate / 1.) CH₂Cl₂, (CCl₄-solid CO₂), 1.25 h, 2.) Et₂O, 0 deg C, 1.5 h

2: 85 percent / sodium periodate / H₂O; methanol / 18 h

3: 44 percent / 3M sulphuric acid / dioxane / 24 h

With sodium periodate; sulfuric acid; chloroformic acid ethyl ester; triethylamine hydrochloride; In 1,4-dioxane; methanol; water;