2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine

Base Information

• Chemical Name: 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine
• CAS No.: 152770-36-0
• Molecular Formula: C₁₅H₁₆N₆O₇
• Molecular Weight: 392.328

Synonyms:2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine

Chemical Property of 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine

Chemical Property:

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Technology Process of 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine

There total 2 articles about 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-nitrobenzenediazonium tetrafluoroborate (365-33-3) + C9H12N3O5(1-)*K(1+) (132658-08-3) → 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine (152770-36-0)

Guidance literature:

In acetone; at 20 ℃; for 18h;

DOI:10.1007/BF00531663

Reference yield:

2-nitrobenzenediazonium tetrafluoroborate (365-33-3) + 5-Nitro-5H-2-acetonyl-4,6-dimethoxy-2,5-dihydropyrimidine (132658-20-9) → 2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine (152770-36-0)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, THF, -78 deg C, 15 min, 2.) hexane, THF, -78 deg C, 2 h;

DOI:10.1007/BF00531663

Reference yield: 82.0%

2-acetonyl-5-nitro-5-(2-nitrophenylazo)-4,6-dimethoxy-2,5-dihydropyrimidine (152770-36-0) → 1-[4,6-Dimethoxy-5-(2-nitro-phenylazo)-pyrimidin-2-yl]-propan-2-one

Guidance literature:

With potassium hydroxide; In methanol; for 2h;

DOI:10.1007/BF00531663

upstream raw materials:

2-nitrobenzenediazonium tetrafluoroborate

5-Nitro-5H-2-acetonyl-4,6-dimethoxy-2,5-dihydropyrimidine

C₉H₁₂N₃O₅^(1-)*K⁽¹⁺⁾

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