(E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

Base Information

Chemical Name:(E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal
CAS No.:882999-61-3
Molecular Formula:C₂₁H₁₇Cl₂NO₅
Molecular Weight:434.276
Hs Code.:

Synonyms:(E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

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Chemical Property of (E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

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Technology Process of (E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

There total 1 articles about (E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 882999-60-2
(E)-3-(2,3-dioxo-2,3-dihydro-1H-indol-7-yl)acrylic acid methyl ester ethylene glycol acetal

: 94-99-5
2,4-Dichlorobenzyl chloride

: 882999-61-3
(E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 50 ℃;

Reference yield: 95.0%

: 882999-61-3
(E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal

: C₂₀H₁₅Cl₂NO₅

Guidance literature:: (E)-3-[1-(2,4-dichlorobenzyl)-2,3-dioxo-2,3-dihydro-1H-indol-7-yl]acrylic acid methyl ester ethylene glycol acetal; With methanol; sodium hydroxide; water; at 5 - 75 ℃; for 4.16667h;

With hydrogenchloride; at 0 ℃; pH=1;