methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

Base Information

Chemical Name:methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate
CAS No.:1448603-36-8
Molecular Formula:C₂₂H₂₄N₄O₄
Molecular Weight:408.457
Hs Code.:

Synonyms:methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

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Chemical Property of methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

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Technology Process of methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

There total 2 articles about methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1448603-16-4
methyl 3-(4-(2-oxo-2-(prop-2-yn-1-ylamino)ethoxy)phenyl)propanoate

: 622-79-7
benzyl azide

: 1448603-36-8
methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

Guidance literature:: With copper(I) oxide; benzoic acid; In water; at 45 ℃; for 4h; Schlenk technique;
DOI:10.1016/j.tetlet.2013.06.051

Reference yield:

: 100613-46-5
3-(4-methoxycarbonylmethoxy-phenyl)-propionic acid methyl ester

: 1448603-36-8
methyl 3-(4-(2-(((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethoxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: CAL-B (Candida antarctica lipase B) immobilized on an acrylic resin (Novozyme? 435) / tert-butyl methyl ether / 4 h / 45 °C / Schlenk technique; Enzymatic reaction

2: copper(I) oxide; benzoic acid / water / 4 h / 45 °C / Schlenk technique

With copper(I) oxide; benzoic acid; In tert-butyl methyl ether; water;
DOI:10.1016/j.tetlet.2013.06.051