C₅₉H₅₅FN₃O₉P

Base Information

Chemical Name:C₅₉H₅₅FN₃O₉P
CAS No.:1445380-31-3
Molecular Formula:C₅₉H₅₅FN₃O₉P
Molecular Weight:1000.07
Hs Code.:

C<sub>59</sub>H<sub>55</sub>FN<sub>3</sub>O<sub>9</sub>P

Synonyms:C₅₉H₅₅FN₃O₉P

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Chemical Property of C₅₉H₅₅FN₃O₉P

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Technology Process of C₅₉H₅₅FN₃O₉P

There total 6 articles about C₅₉H₅₅FN₃O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1445380-21-1
C₅₁H₄₈FN₃O₆

: 192752-93-5
3-methylsalicylchlorophosphane

: 1445380-31-3
C₅₉H₅₅FN₃O₉P

Guidance literature:: C₅₁H₄₈FN₃O₆; 3-methylsalicylchlorophosphane; In acetonitrile; at 0 - 20 ℃; for 2h; Inert atmosphere;

With iodine; In pyridine; dichloromethane; water; acetonitrile; for 0.5h;

Reference yield:

: 2-chloro-8-methyl-(4H)-1,3,2-benzodioxaphosphorin-2-oxide

: 1445380-21-1
C₅₁H₄₈FN₃O₆

: 1445380-31-3
C₅₉H₅₅FN₃O₉P

Guidance literature:: 2-chloro-8-methyl-(4H)-1,3,2-benzodioxaphosphorin-2-oxide; C₅₁H₄₈FN₃O₆; With 1-methyl-1H-imidazole; In acetonitrile; at 0 - 20 ℃; for 2h; Inert atmosphere;

With pyridine; iodine; In dichloromethane; water; acetonitrile; for 0.5h;

Reference yield:

: C₂₇H₃₄FN₃O₄Si

: 1445380-31-3
C₅₉H₅₅FN₃O₉P

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,4,6-trimethyl-pyridine; silver nitrate / dichloromethane / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 - 45 °C

3.1: 1-methyl-1H-imidazole / acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0.5 h

With 1-methyl-1H-imidazole; 2,4,6-trimethyl-pyridine; tetrabutyl ammonium fluoride; silver nitrate; In tetrahydrofuran; dichloromethane; acetonitrile;