3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI)

Base Information

Chemical Name:3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI)
CAS No.:727985-40-2
Molecular Formula:C₁₀H₁₅NO
Molecular Weight:165.235
Hs Code.:
Mol file:727985-40-2.mol

Synonyms:3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI)

Chemical Property:

Purity/Quality:

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Technology Process of 3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI)

There total 4 articles about 3(2H)-Indolizinone,hexahydro-5-methyl-7-methylene-,(5R,8aR)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-ethoxy-N-((1R)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 727985-40-2,727985-41-3
(5R,9R)-5-methyl-7-methyleneindolizidin-one

: 727985-40-2
(5R,9S)-5-methyl-7-methyleneindolizidin-one

Guidance literature:: 5-ethoxy-N-((1R)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one; (trimethylsilyl)methylmagnesium chloride; With cerium(III) chloride; In tetrahydrofuran; at 20 ℃; for 72h;

With hydrogenchloride; at 0 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/np049902u

Reference yield:

: 5-ethoxy-N-((1R)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 727985-40-2,727985-41-3
(5R,9R)-5-methyl-7-methyleneindolizidin-one

: 727985-40-2
(5R,9S)-5-methyl-7-methyleneindolizidin-one

Guidance literature:: 5-ethoxy-N-((1R)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one; (trimethylsilyl)methylmagnesium chloride; With cerium(III) chloride; In tetrahydrofuran; at 20 ℃; for 72h;

With hydrogenchloride; at 0 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/np049902u

Reference yield:

: 5-ethoxy-N-((1S)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 727985-40-2
(5S,9R)-5-methyl-7-methyleneindolizidin-one

: 727985-40-2
(5S,9S)-5-methyl-7-methyleneindolizidin-one

Guidance literature:: 5-ethoxy-N-((1S)-methyl-2-ethoxycarbonylethyl)pyrrolidin-2-one; (trimethylsilyl)methylmagnesium chloride; With cerium(III) chloride; In tetrahydrofuran; at 20 ℃; for 72h;

With hydrogenchloride; at 0 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1021/np049902u