benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Base Information

Chemical Name:benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate
CAS No.:1620620-29-2
Molecular Formula:C₁₅H₁₉NO₇S
Molecular Weight:357.384
Hs Code.:

Synonyms:benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Suppliers and Price of benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

There total 4 articles about benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₉NO₆S

: 1620620-29-2
benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Guidance literature:: With sodium periodate; ruthenium(III) trichloride hydrate; In water; acetonitrile; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c4ob01047g

Reference yield:

: 59524-02-6,145612-59-5,141527-78-8
(R)-benzyl 2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

: 1620620-29-2
benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / dichloromethane / 0.5 h / -40 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: ruthenium(III) trichloride hydrate; sodium periodate / acetonitrile; water / 1 h / 0 °C / Inert atmosphere

With sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; In dichloromethane; water; acetonitrile;
DOI:10.1039/c4ob01047g

Reference yield:

: C₈H₁₄NO₅^(1-)*K⁽¹⁺⁾

: 1620620-29-2
benzyl (4R)-3-(tert-butyloxycarbonyl)-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 16 h / 20 °C

2: thionyl chloride; pyridine / acetonitrile / 3.5 h / -42 °C / Inert atmosphere

3: sodium periodate; ruthenium(III) trichloride hydrate / water; acetonitrile / 4.25 h / 0 - 20 °C

With pyridine; sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2014.07.023