Technology Process of (1S,2S,3R,4R,6S)-4-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclohexane-1,2,3-triyl triacetate
There total 3 articles about (1S,2S,3R,4R,6S)-4-(acetoxymethyl)-6-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclohexane-1,2,3-triyl triacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 6h;
Reagent/catalyst;
Solvent;
Time;
Inert atmosphere;
DOI:10.1002/ejoc.201301874
- Guidance literature:
-
Multi-step reaction with 3 steps
1: imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(ll) sulfate pentahydrate / methanol / 12 h / 20 °C
2: sodium L-ascorbate / N,N-dimethyl-formamide / 8 h / 100 °C / Inert atmosphere
3: dmap / N,N-dimethyl-formamide / 6 h / Inert atmosphere
With
dmap; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301874
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / 20 °C
2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 6 h / 100 °C / Inert atmosphere
With
copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
pyridine; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301874
