Technology Process of C34H44N4O5S2
There total 13 articles about C34H44N4O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
at 120 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: ammonia / methanol / 15 h
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice
2.2: 0.17 h / -78 °C
3.1: sodium ethanolate / ethanol / 16 h / 0 - 20 °C / Cooling with ice
4.1: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 6 h / 27 °C
5.1: thionyl chloride; N,N-dimethyl-formamide / benzene / 20 °C / Inert atmosphere
5.2: 0 °C
6.1: diisobutylaluminium hydride / dichloromethane / 0.75 h / -78 °C
6.2: 12 h / 27 °C
7.1: potassium carbonate / 1 h / 120 °C
With
thionyl chloride; oxalyl dichloride; lithium hydroxide monohydrate; ammonia; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 6 h / 27 °C
2.1: thionyl chloride; N,N-dimethyl-formamide / benzene / 20 °C / Inert atmosphere
2.2: 0 °C
3.1: diisobutylaluminium hydride / dichloromethane / 0.75 h / -78 °C
3.2: 12 h / 27 °C
4.1: potassium carbonate / 1 h / 120 °C
With
thionyl chloride; lithium hydroxide monohydrate; diisobutylaluminium hydride; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; water; benzene;
