methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

Base Information

Chemical Name:methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride
CAS No.:948992-53-8
Molecular Formula:C₁₂H₁₈N₂O₄S*ClH
Molecular Weight:322.813
Hs Code.:

Synonyms:methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

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Chemical Property of methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

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Technology Process of methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

There total 5 articles about methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 918813-13-5
Methyl 3-cyano-4-(isopropylsulfonyl)phenylcarbamate

: 948992-53-8
methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

Guidance literature:: Methyl 3-cyano-4-(isopropylsulfonyl)phenylcarbamate; With hydrogen; nickel; In tetrahydrofuran; for 6h; under 3102.97 Torr;

With hydrogenchloride; In 1,4-dioxane; diethyl ether;

Reference yield:

: 918813-12-4
5-amino-2-(isopropylsulfonyl)benzonitrile

: 948992-53-8
methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2.33 h / 0 - 20 °C

2: hydrogen / nickel / tetrahydrofuran / 6 h / 3102.97 Torr

With pyridine; hydrogen; nickel; In tetrahydrofuran;

Reference yield:

: 17417-09-3
2-fluoro-5-nitrobenzonitrile

: 948992-53-8
methyl 3-(aminomethyl)-4-(isopropylsulfonyl)phenylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C

3: hydrogen / palladium on activated charcoal / tetrahydrofuran / 2585.81 Torr

4: pyridine / 2.33 h / 0 - 20 °C

5: hydrogen / nickel / tetrahydrofuran / 6 h / 3102.97 Torr

With pyridine; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; nickel; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;