C₂₂H₂₈O₂

Base Information

• Chemical Name: C₂₂H₂₈O₂
• CAS No.: 1163790-51-9
• Molecular Formula: C₂₂H₂₈O₂
• Molecular Weight: 324.463
• Mol file: 1163790-51-9.mol

Synonyms:C₂₂H₂₈O₂

Chemical Property of C₂₂H₂₈O₂

Chemical Property:

Purity/Quality:

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Technology Process of C₂₂H₂₈O₂

There total 2 articles about C₂₂H₂₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-tert-butoxystyrene (95418-58-9) → C22H28O2 (1163790-51-9)

Guidance literature:

With silica immobilized second generation Hoveyda-Grubbs catalyst; In hexane; at 59.84 ℃; for 5h;

DOI:10.1002/adsc.200800211

Reference yield:

p-tert-butoxybenzaldehyde (57699-45-3) → C22H28O2 (1163790-51-9) + C22H28O2

Guidance literature:

With 4-methylbenzylthiol; catalyst; caesium carbonate; bis(pinacol)diborane; In N,N-dimethyl-formamide; at 25 ℃; for 24h; Overall yield = 42 %; diastereoselective reaction; Irradiation; Inert atmosphere;

DOI:10.1039/c9sc00711c

upstream raw materials:

4-tert-butoxystyrene

p-tert-butoxybenzaldehyde