Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)

Base Information

Chemical Name:Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)
CAS No.:727654-69-5
Molecular Formula:C9H14 N2 O
Molecular Weight:166.223
Hs Code.:

Synonyms:Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)

Suppliers and Price of Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)

Chemical Property:

PSA：32.67000
LogP:1.21320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI)

There total 5 articles about Methanimidamide, N,N-dimethyl-N-(3-oxo-1-cyclohexen-1-yl)-, [N(E)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5220-49-5
3-amino-cyclohex-2-enone

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 727654-69-5
3-(4α-N,N-dimethylaminomethylene)amino-2-cyclohexen-1-one

Guidance literature:: 3-amino-cyclohex-2-enone; N,N-dimethyl-formamide dimethyl acetal; In tetrahydrofuran; for 2.5h; Heating;

In toluene; for 1h; Further stages.; Heating;
DOI:10.1016/j.tetlet.2004.04.123

Reference yield: 60.0%

: 5220-49-5
3-amino-cyclohex-2-enone

: 1188-33-6
N,N-dimethylformamide diethyl diacetal

: 727654-69-5
3-(4α-N,N-dimethylaminomethylene)amino-2-cyclohexen-1-one

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1007/BF00767027

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 727654-69-5
3-(4α-N,N-dimethylaminomethylene)amino-2-cyclohexen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / NH₄OAc / toluene / 5 h / Heating

2.1: tetrahydrofuran / 2.5 h / Heating

2.2: 92 percent / toluene / 1 h / Heating

With ammonium acetate; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetlet.2004.04.123