4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine

Base Information

Chemical Name:4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine
CAS No.:180207-94-7
Molecular Formula:C₁₅H₁₇ClN₂O₂
Molecular Weight:292.765
Hs Code.:
DSSTox Substance ID:DTXSID901184303

Synonyms:DTXSID901184303;4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine;180207-94-7

Suppliers and Price of 4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:292.0978555
Heavy Atom Count:20
Complexity:293

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CNC2=C(C=CC(=C2)Cl)N)OC

Technology Process of 4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine

There total 3 articles about 4-Chloro-N2-[(3,4-dimethoxyphenyl)methyl]-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 180207-93-6
3-chloro-N-(3,4-dimethoxybenzyl)-6-nitroaniline

: 180207-94-7
4-Chloro-N²-(3,4-dimethoxy-benzyl)-benzene-1,2-diamine

Guidance literature:: With hydrogen; Pt(S)/C; In ethanol; for 16h; under 1551.4 Torr;
DOI:10.1021/jm960070+

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 180207-94-7
4-Chloro-N²-(3,4-dimethoxy-benzyl)-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / EtNiPr₂ / 408 h / 75 °C

2: 96 percent / H₂ / Pt/S/C / ethanol / 16 h / 1551.4 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; Pt(S)/C; In ethanol;
DOI:10.1021/jm960070+

Reference yield:

: 5763-61-1
3,4-dimethoxybenzylamine

: 180207-94-7
4-Chloro-N²-(3,4-dimethoxy-benzyl)-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / EtNiPr₂ / 408 h / 75 °C

2: 96 percent / H₂ / Pt/S/C / ethanol / 16 h / 1551.4 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; Pt(S)/C; In ethanol;
DOI:10.1021/jm960070+