C₂₂H₂₉NO₆

Base Information

Chemical Name:C₂₂H₂₉NO₆
CAS No.:943542-53-8
Molecular Formula:C₂₂H₂₉NO₆
Molecular Weight:403.475
Hs Code.:

C<sub>22</sub>H<sub>29</sub>NO<sub>6</sub>

Synonyms:C₂₂H₂₉NO₆

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Chemical Property of C₂₂H₂₉NO₆

Chemical Property:

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Technology Process of C₂₂H₂₉NO₆

There total 17 articles about C₂₂H₂₉NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 943542-52-7
C₂₇H₃₇NO₆

: 943542-53-8
C₂₂H₂₉NO₆

Guidance literature:: With 1.3-propanedithiol; hydrogenchloride; In 2,2,2-trifluoroethanol; at 60 ℃; for 4h;
DOI:10.1021/ol0706051

Reference yield:

: 943542-50-5
C₁₅H₂₃NO₆

: 943542-53-8
C₂₂H₂₉NO₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: 8.8 g / t-BuOK / tetrahydrofuran / 6 h / 20 °C

2.1: lithium borohydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: tetrahydrofuran; methanol / 24 h / 20 °C

3.1: 3.9 g / NMO; TPAP / CH₂Cl₂ / 18 h / 20 °C

4.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

4.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

5.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

6.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

7.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

8.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

With 1.3-propanedithiol; hydrogenchloride; sodium tetrahydroborate; lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; potassium tert-butylate; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1021/ol0706051

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 943542-53-8
C₂₂H₂₉NO₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 48 h / 20 °C

2.1: tetrahydrofuran / 11.5 h / -78 - 20 °C

2.2: 80.4 percent / ethanolamine / tetrahydrofuran / 8 h / 20 °C

3.1: aq. HCl / tetrahydrofuran / 10 h / 60 °C

4.1: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 20 °C

5.1: 136 mg / triethylamine / CH₂Cl₂ / 10 h / 20 °C

6.1: 94 percent / 1,3-propanedithiol; aq. HCl / 2,2,2-trifluoro-ethanol / 4 h / 60 °C

With 1.3-propanedithiol; hydrogenchloride; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1021/ol0706051