ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

Base Information

Chemical Name:ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate
CAS No.:1454907-80-2
Molecular Formula:C₁₆H₁₈NO₂P
Molecular Weight:287.298
Hs Code.:

Synonyms:ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

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Chemical Property of ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

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Technology Process of ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

There total 1 articles about ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 181515-26-4
(1-phenylethenyl)phosphonic acid monoethyl ester

: 62-53-3
aniline

: 1454907-80-2
ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

Guidance literature:: (1-phenylethenyl)phosphonic acid monoethyl ester; With N,N-diethyl-1,1,1-trimethylsilanamine; In dichloromethane; at 20 ℃; for 1h;

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 3h;

aniline; With triethylamine; In acetonitrile; at 50 ℃; for 1h;
DOI:10.1039/c3cc44995e

Reference yield: 64.0%

: 1454907-80-2
ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

: 22979-35-7
Methyl phenyldiazoacetate

: C₂₅H₂₆NO₄P

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 60 ℃; for 2h;
DOI:10.1002/bkcs.12040

Reference yield: 54.0%

: 1454907-80-2
ethyl N-phenyl-P-(1-phenylvinyl)phosphonamidate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: methyl 2-(1-ethoxy-2,5-diphenyl-2,3-dihydro-1H-2,1-azaphosphol-3-yl-1-oxide)acetate

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; caesium carbonate; In 1,2-dichloro-ethane; at 80 ℃; for 30h;
DOI:10.1039/c3cc44995e