Technology Process of C12H7F6N
There total 3 articles about C12H7F6N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Trifluoromethanesulfonamide; (IPr)Au(NTf2);
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
DOI:10.1039/c4cc00493k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / Inert atmosphere
2: hydroxylamine hydrochloride; triethylamine / dichloromethane / 24 h / 0 °C / Inert atmosphere
3: (IPr)Au(NTf2); Trifluoromethanesulfonamide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; Trifluoromethanesulfonamide; (IPr)Au(NTf2); hydroxylamine hydrochloride; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
1: |Sonogashira Cross-Coupling;
DOI:10.1039/c4cc00493k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; triethylamine / dichloromethane / 24 h / 0 °C / Inert atmosphere
2: (IPr)Au(NTf2); Trifluoromethanesulfonamide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With
Trifluoromethanesulfonamide; (IPr)Au(NTf2); hydroxylamine hydrochloride; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc00493k