3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI)

Base Information

Chemical Name:3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI)
CAS No.:727428-90-2
Molecular Formula:C₈H₁₂O₃
Molecular Weight:156.181
Hs Code.:
Mol file:727428-90-2.mol

Synonyms:3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI)

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Chemical Property of 3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI)

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Technology Process of 3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI)

There total 10 articles about 3-Oxabicyclo[3.2.0]heptane-2-carboxylicacid,methylester,(1R,2R,5S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-(1R,2R,5S)-1-(3-Oxa-bicyclo[3.2.0]hept-2-yl)-ethane-1,2-diol

: 727428-91-3,727428-90-2
(1R,2R,5S)-3-oxabicyclo[3.2.0]heptane-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium metaperiodate; RuCl₃*3H₂O / CCl₄; H₂O; acetonitrile / 1.5 h / 20 °C

2: 200 mg / diethyl ether

With ruthenium trichloride; sodium periodate; In tetrachloromethane; diethyl ether; water; acetonitrile;

Reference yield:

: 727428-84-4
(2R)-2-[(1R,2R,5S)-3-oxabicyclo[3.2.0]hept-2-yl]-1,4-dioxa-spiro[4.5]decane

: 727428-91-3,727428-90-2
(1R,2R,5S)-3-oxabicyclo[3.2.0]heptane-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / H₂O / 24 h / 20 °C

2: sodium metaperiodate; RuCl₃*3H₂O / CCl₄; H₂O; acetonitrile / 1.5 h / 20 °C

3: 200 mg / diethyl ether

With ruthenium trichloride; sodium periodate; acetic acid; In tetrachloromethane; diethyl ether; water; acetonitrile;

Reference yield:

: (R)-(1S,2S,5R)-1-(3-Oxa-bicyclo[3.2.0]hept-2-yl)-ethane-1,2-diol

: 727428-91-3,727428-90-2
(1S,2S,5R)-3-oxabicyclo[3.2.0]heptane-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium metaperiodate / RuCl₃*xH₂O / acetonitrile; CCl₄; H₂O / 20 °C

2: diethyl ether

With sodium periodate; ruthenium trichloride; In tetrachloromethane; diethyl ether; water; acetonitrile;
DOI:10.1021/ol049696h