bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane

Base Information

• Chemical Name: bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane
• CAS No.: 1430802-64-4
• Molecular Formula: C₂₉H₃₄BBr₂NO₂
• Molecular Weight: 599.213
• Mol file: 1430802-64-4.mol

Synonyms:bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane

Chemical Property of bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane

There total 1 articles about bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

tert-butyl carbazate (4248-19-5) + tris(4-bromo-2,6-dimethylphenyl)-borane (1239448-99-7) → bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane (1430802-64-4)

Guidance literature:

With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; for 24h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2013.03.080

Reference yield: 99.0%

bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane (1430802-64-4) → 4-amino-2,6-dimethylphenylbis(4-bromo-2,6-dimethylphenyl)borane (1430802-65-5)

Guidance literature:

bis(4-bromo-2,6-dimethylphenyl)[4-(tert-butoxycarbonylamino)-2,6-dimethylphenyl]borane; With hydrogenchloride; In 1,4-dioxane; chloroform; at 20 ℃; for 5h; Inert atmosphere;

With water; sodium hydrogencarbonate; pH=8; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.03.080

upstream raw materials:

tert-butyl carbazate

tris(4-bromo-2,6-dimethylphenyl)-borane

Downstream raw materials:

4-amino-2,6-dimethylphenylbis(4-bromo-2,6-dimethylphenyl)borane