[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]

Base Information

• Chemical Name: [Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]
• CAS No.: 85837-43-0
• Molecular Formula: BF₄*C₄₃H₃₆ClIrN₃O₃P₂
• Molecular Weight: 1019.2

Synonyms:[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]

Chemical Property of [Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]

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Technology Process of [Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]

There total 1 articles about [Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Ir(NHNHC6H3NO2-o)(CO)(PPh3)2][BF4] → [Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2][BF4] (85837-43-0)

Guidance literature:

With HCl; In chloroform; adding of freshly-made HCl solution in CHCl3 under N2 or HCl bubbling through CHCl3 solution of starting complex in a foil-wrapped Schlenk tube; pptn. with diethyl ether, washing twice with ether, vac. drying, elem. anal.;

DOI:10.1016/S0022-328X(00)98635-2

Reference yield:

[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2][BF4] (85837-43-0) → [Ir(NHNHC6H3NO2-o)(CO)(PPh3)2][BF4]

Guidance literature:

With CH₃OH;

DOI:10.1016/S0022-328X(00)98635-2

Reference yield:

[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2][BF4] (85837-43-0) → [Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2][BF4] (85837-45-2)

Guidance literature:

With HCl; liq. HCl action;

DOI:10.1016/S0022-328X(00)98635-2

Downstream raw materials:

[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]

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