C₃₂H₄₇N₃O₈

Base Information

Chemical Name:C₃₂H₄₇N₃O₈
CAS No.:1403482-51-8
Molecular Formula:C₃₂H₄₇N₃O₈
Molecular Weight:601.74
Hs Code.:

C<sub>32</sub>H<sub>47</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₂H₄₇N₃O₈

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Chemical Property of C₃₂H₄₇N₃O₈

Chemical Property:

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Technology Process of C₃₂H₄₇N₃O₈

There total 6 articles about C₃₂H₄₇N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₂H₃₀INO₆

: 109838-85-9
(2R)-2,5-dihydro-2-isopropyl-3,6-dimethoxypyrazine

: 1403482-51-8
C₃₂H₄₇N₃O₈

Guidance literature:: (2R)-2,5-dihydro-2-isopropyl-3,6-dimethoxypyrazine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

With copper(l) cyanide; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.025h; Inert atmosphere;

C₂₂H₃₀INO₆; In tetrahydrofuran; hexane; at -78 - -25 ℃; for 16.5h; Inert atmosphere;
DOI:10.1021/ja307060p

Reference yield:

: 1431134-87-0
C₂₃H₃₁NO₇

: 1403482-51-8
C₃₂H₄₇N₃O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; sodium sulfite; sodium iodide / acetone / 3 h / 50 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

4.2: 0.03 h / -78 - 0 °C / Inert atmosphere

4.3: 16.5 h / -78 - -25 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; sodium hydrogencarbonate; triethylamine; sodium iodide; sodium sulfite; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone;
DOI:10.1021/ja307060p

Reference yield:

: 1403482-38-1
C₂₂H₃₃NO₈

: 1403482-51-8
C₃₂H₄₇N₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 22 °C

1.2: 20 h

2.1: iodine / acetone / 0.33 h / 20 °C

3.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; sodium sulfite; sodium iodide / acetone / 3 h / 50 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

6.2: 0.03 h / -78 - 0 °C / Inert atmosphere

6.3: 16.5 h / -78 - -25 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; iodine; sodium hydride; sodium hydrogencarbonate; triethylamine; sodium iodide; sodium sulfite; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone;
DOI:10.1021/ja307060p