2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

Base Information

Chemical Name:2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester
CAS No.:220446-56-0
Molecular Formula:C₂₉H₄₉O₉P
Molecular Weight:572.676
Hs Code.:

Synonyms:2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

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Chemical Property of 2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

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Technology Process of 2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

There total 7 articles about 2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Dodecanoic acid (R)-2-benzyloxy-3-[((S)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-methoxy-phosphanyloxy]-propyl ester

: 220446-56-0
2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -20 - 0 ℃; for 0.5h;
DOI:10.1021/jo981653p

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 220446-56-0
2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / (dimethylamino)pyridine / dimethylformamide / 0.75 h / 5 °C

2: NaHCO₃; NaIO₄ / CH₂Cl₂; ethanol; H₂O / 2.5 h / 20 °C

3: 1.60 g / NaBH₃CN; acetic acid / methanol; H₂O / 1.5 h / 20 °C

4: 1H-tetrazole / CH₂Cl₂ / 2 h / 0 °C

5: 1H-tetrazole / CH₂Cl₂ / 2 h / 0 °C

6: 4.7 g / m-CPBA / CH₂Cl₂ / 0.5 h / -20 - 0 °C

With 1H-tetrazole; dmap; sodium periodate; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 1: Acylation / 2: Oxidation / 3: Reduction / 4: Condensation / 5: Condensation / 6: Oxidation;
DOI:10.1021/jo981653p

Reference yield:

: 17618-04-1
2,5-di-O-benzyl-D-mannitol

: 220446-56-0
2-benzyl-1-lauroyl-sn-glycero-3-[phospho-1-isopropylideneglycerol] methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / (dimethylamino)pyridine / dimethylformamide / 0.75 h / 5 °C

2: NaHCO₃; NaIO₄ / CH₂Cl₂; ethanol; H₂O / 2.5 h / 20 °C

3: 1.60 g / NaBH₃CN; acetic acid / methanol; H₂O / 1.5 h / 20 °C

4: 1H-tetrazole / CH₂Cl₂ / 2 h / 0 °C

5: 1H-tetrazole / CH₂Cl₂ / 2 h / 0 °C

6: 4.7 g / m-CPBA / CH₂Cl₂ / 0.5 h / -20 - 0 °C

With 1H-tetrazole; dmap; sodium periodate; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 1: Acylation / 2: Oxidation / 3: Reduction / 4: Condensation / 5: Condensation / 6: Oxidation;
DOI:10.1021/jo981653p