N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

Base Information Edit

Chemical Name:N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester
CAS No.:32402-31-6
Molecular Formula:C₁₆H₂₂N₂O₅
Molecular Weight:322.361
Hs Code.:
Mol file:32402-31-6.mol

Synonyms:N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

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Chemical Property of N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

There total 2 articles about N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1149-26-4,1685-33-2,92077-76-4,3588-63-4
N-benzyloxycarbonylvaline

: 616-34-2
methoxycarbonylmethylamine

: 32402-31-6
N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

Guidance literature:: With 4-methyl-morpholine; DMT*brucine tetrafluoroborate; brucine; In acetonitrile; at 0 - 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol802691x

Reference yield: 87.0%

: 1685-33-2
N-[(benzyloxy)carbonyl]-D-valine

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 32402-31-6
N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/P19950000157

Reference yield: 53.0%

: 32402-31-6
N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester

: 143673-66-9
(R)-3-(1-methylethyl)-piperazine-2,5-one

Guidance literature:: N-benzyloxycarbonyl-(2R)-valinylglycine methyl ester; With 5%-palladium/activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 2h; under 775.743 Torr;

In toluene; at 110 - 130 ℃; for 20h;