2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol

Base Information

• Chemical Name: 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol
• CAS No.: 1402436-31-0
• Molecular Formula: C₂₃H₂₇BrO₆
• Molecular Weight: 479.368

Synonyms:2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol

Chemical Property of 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol

Chemical Property:

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Technology Process of 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol

There total 6 articles about 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5-(1-benzyloxy-2-trityloxyethyl)-6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole (1402436-30-9) → 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol (1402436-31-0)

Guidance literature:

With water; acetic acid; at 60 ℃; for 10h;

DOI:10.1002/adsc.201100988

Reference yield:

1-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]-2-trityloxyethanol (1402436-26-3) → 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol (1402436-31-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 0 - 20 °C

1.2: 20 °C

2.1: water; acetic acid / 10 h / 60 °C

With tetrabutylammomium bromide; water; acetic acid; sodium hydroxide; In dichloromethane;

DOI:10.1002/adsc.201100988

Reference yield:

1-Bromo-2-bromomethyl-benzene (3433-80-5) → 2-benzyloxy-2-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]ethanol (1402436-31-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 0 - 20 °C

1.2: 20 °C

2.1: water; acetic acid / 8 h / 20 °C

3.1: pyridine / 10 h / 60 °C

4.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 0 - 20 °C

4.2: 20 °C

5.1: water; acetic acid / 10 h / 60 °C

With pyridine; tetrabutylammomium bromide; water; acetic acid; sodium hydroxide; In dichloromethane;

DOI:10.1002/adsc.201100988

upstream raw materials:

1-[6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl]-2-trityloxyethanol

5-(1-benzyloxy-2-trityloxyethyl)-6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole

1-(6-(2-bromobenzyloxy)tetrahydro-2,2-dimethylfuro[3,2-d][1,3]dioxol-5-yl)ethane-1,2-diol

(3aR,5R,6S,6aR)-6-(2-bromo-benzyloxy)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

Downstream raw materials:

C₂₆H₂₈O₆

5-(1-benzyloxy-2-prop-2-ynyloxyethyl)-6-(2-bromobenzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole

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